IKA RV 10.1 Mounting Instruction

MontageanleitungMounting instructionInstruction de montageИнструкция по монтажу20000005212RV 10_1_2_10_20_042016Betriebsanleitung DEOperating instructions ENMode d’emploi FRИнструкция по монтажу RU00/0000/0IKA® - Werke GmbH & Co.KGJanke & Kunkel-Str. 10D-79219 StaufenTel. +49 7633 831-0Fax +49 7633 831-98sales@ika.dewww.ika.comEN• Read the mounting instruction in full before starting up and follow the safety instructions.• Refer also to the safety instructions of operating instructions for the manual of the rotary evaporator.• Keep the operating instructions in a place where they can be accessed by everyone.• Ensure that only trained staff work with the appliance.• Follow the safety instructions, guidelines, occupational health and safety and accident prevention regulations. When working under a vacuum in particular!• Wear your personal protective equipment in accordance with the hazard category of the medium to be processed. Otherwise there is a risk of:- splashing liquids,- body parts, hair, clothing and jewellery getting caught,- injury as a result of glass breakage.• Ensure that there is sufficient space above the device as the glass assembly may exceed the height of the device.• Prior to each use, always check the device, accessories and especially the glass parts for damage. Do not use damaged components.• Ensure that the glass assembly is tension-free! Danger of cracking as a result of:- stress due to incorrect assembly,- external mechanical hazards,- local temperature peaks.• Operation with excess pressure is not permitted (cooling water pressure 0.5 bar, minimum cooling water flow rate 30 l/h, maximum cooling water flow rate 100 l/h).• The glass equipment must always be ventilated when working under normal pressure (e.g. open outlet at cooler) in order to prevent a pressure build-up.• Evacuated glass vessels must not be heated on one side; the evaporating flask must rotate during the heating phase.• The glassware is designed for operation under a vacuum of up to 1 mbar. The equipment must be evacuated prior to heating (see manual rotation drive,chapter ”Commissioning”). The equipment must only be aired again after cooling. When carrying out vacuum distillation, uncondensed vapours mustbe condensed out or safely dissipated. If there is a risk that the distillation residue could disintegrate in the presence of oxygen, only inert gas must beadmitted for stress relief.• Danger of burning! The heating bath, tempering medium, evaporator piston and glass assembly can become hot during operation and remain sofor a long time afterwards! Let the components cool off before continuing work with the device.• A vacuum may form inside the glassware in case of power outage of the rotation drive.• Imbalance may result in uncontrolled resonance behaviour of the rotation drive or the assembly. Glass apparatus may be damaged or destroyed. In theevent of unbalance or unusual noises, switch off the rotation drive immediately or reduce the speed.• Caution! The surface of the evaporating flask is slippery when silicone oil is used as a tempering medium in the heating bath!The glassware is made of borosilicate glass 3.3.The coating of the glassware vertical coated is made out of the material SURLYN.The glassware vertical coated by SURLYN are suitable for the use in a temperature range from -30 upto +60 °C.Item Designation Quantity glassware diagonal Quantity glassware vertical1 Receiving flask 1 12 Clamp NS 29, stainless steel 1 14 Stopcock 1 15 Tube - 16 Condenser 1 Diagonal condenser 1 Vertical condenser7 Connection 1 Introduction sleeve 1 Vacuum connection8 Clamp NS 29, plastic 1 110 Evaporator piston 1000 ml 1 111 Ball joint clamp RV 05.10 1 112 Screw joint cap 4 413 Hose connection 4 418 Washer - 1Safety instructionsProduct informationDelivery scopeMounting vacuum seal (illustrations zoomed in see manual rotary evaporator)Inserting vacuum seal Place the vacuum seal in the condenserreceptacle and fit the glassware to thedevice according to the assembly inst-ructions (Fig. 11 a, b and c).Note: The vacuum seal has to be intro-duced completely into the the condenserreceptacle. Pay attention to the correctpositon of the vacuum seal.First use Insert steam tube (1). Insert the vacuum seal (2). Pay attention tothe correct positon of the vacuum seal! Loosen the union nut and the annular springfrom the drive head of the rotation evapora-tor and slide these parts over the condenserflange (Fig. 11d). The annular spring engagesin the flange slot, so the union nut is secured. Mount the small parts onto the condenser. Secure the vertical condenser by the Velcro ®band to the support rod.Hinweis: See operating instructions for the rotaryevaporator!123a3bFig. 11aFig. 11bFig. 11cFig. 11dThe seal on the glass condenser should be checked at regular intervals and replaced if necessary.For cleaning disconnect the main plug.To clean the glassware use only water with a detergent that contains tensides, or use isopropylalcohol for stubborn soiling.CleaningSource language: GermanGlassatz vertikal /Glassware vertical /Verrerie verticale /Вертикальная стеклянная посудаRV 10.1RV 10.700RV 10.900RV 10.6000Glassatz vertikal beschichtet /Glassware vertical, coated /Verrerie verticale, avec revêtement /Вертикальная стеклянная посудас покрытиемRV 10.10RV 10.710RV 10.910RV 10.6010Glassatz diagonal /Glassware diagonal /Verrerie diagonale /Диагональная стеклянная посудаRV 10.2RV 10.800RV 10.1000RV 10.7000Glassatz diagonal beschichtet /Glassware diagonal, coated /Verrerie diagonale, avec revêtement/ /Диагональная стеклянная посудас покрытиемRV 10.20RV 10.810RV 10.1010RV 10.70107813 (4x)12 (4x)61854111102RotationsantriebRotation driveEntraînement de rotationПривод7813 (4x)12 (4x)61854111102Mounting the washer (illustrations zoomed in see manual rotary evaporator)Fig. 18aDrainagewasherFig. 18bNote:Pay attention to the correct positon of the washer.The PTFE tube (5) with the washer (18) can be mounted optionally on thevertical glass sets.It serves for filling the evaporator flask when there is a vacuum in the glassset.Solvent can be sucked through the PTFE tube into the evaporator flask byopening the stopcock (4).3991500d

/ 2

Related manuals for IKA RV 10.1