Axis ATS60 User Manual
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Contents
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USER MANUAL 2714. Proper moistureBefore measurement carefully prepare the sample (as described in chapter Descriptionof Thermogravimetric Analysis) and set correct drying parameters (see the diagram inchapter 11.6, description of the way of settting is in 11.4).Place an empty single-use pan andtare the balance withT key.The indication should be m=0,000g.Open the drying chamber and usingthe pan handle place the single-usepan with the sample on the pansupport. Close the chamber.Start the measurement choosingSTART key.In the lower line the time left to endthe measurement and successivemeasurement number is displayed.Drying in progress is signalised withalternating SAMPLE /DRYINGcommunicate.Wait until END communicateappears. Now read the result.Attention: No STB communicate and m0 sign in negative, marks acceptance of unstableinitial mass value m0, caused by pressing the pan to chamber wall or by too fast sampledrying, which can cause to measurement failures.m0-m/m0*100% Td=120C ts= 1sekT = 80.23Ct =0:00:00sm= 1.020gm0= 1.020gCSD 00:02:00s0.00 %STARTm0-m/m0*100% Td=120C ts= 1sekT = 80.23Ct =0:00:00sm= 1.020gm0= 1.020gCSD 00:01:29s nr drying/sample0.00 %m0-m/m0*100% Td=120C ts= 1sekT = 80.23Ct =0:00:00sm= 1.020gm0= 1.020gCSD 00:01:29s end1.00 % |
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